Miguel Palma Lovillo

Miguel Palma Lovillo

Prof. Miguel Palma Lovillo

Institution

University of Cádiz, Spain

Area of Research/Interest

Chemometrics, Analytical Chemistry, Functional Foods

Education

1998
PostDoc Analytical Chemistry, Virginia Tech. VA. USA
1995
S3 (Doctor) Sciences, University of Cádiz, Spain
1992
S2 (Master) Analytical Chemistry,University of Cádiz, Spain
1985-1990
S1 (Bachelor) Chemistry, University of Cádiz, Spain

Research Experience

2019-till date
CTQ2017-86661-R Impregnation of extracts and functionalization of antioxidant nanoparticles obtained from mango leaves by using high-pressure techniques and their application in biomedicine
2015-2018
CTQ2014-52427-R Supercritical Impregnation of natural extracts for food preservation
2013-2015
CTQ2011-22974 Fractionation and Purification of antioxidant compounds from
agricultural by-products by using high-pressure separation techniques

Publication (in the last 5 years)

2019
Setyaningsih, W., Majchrzak, T., Dymerski, T., Namieśnik, J., Palma, M. Key-marker volatile compounds in aromatic rice (Oryza sativa) grains: An HS-SPME extraction method combined with GC×GC-TOFMS. (2019) Molecules 24(22):1-15
2019
Vázquez-Espinosa, M., De Peredo, A.V.G., Ferreiro-González, M., Barroso, C.G., Palma, M., Barbero, G.F., Espada-Bellido, E. Optimizing and comparing ultrasound- And microwave-assisted extraction methods applied to the extraction of antioxidant capsinoids in peppers. (2019) Agronomy 9:663 DOI: 10.3390/agronomy9100633
2019
Nebo, L., Varela, R.M., Fernandes, J.B., Palma, M. Microwave-assisted extraction of Ricinine from Ricinus communis leaves. (2019) Antioxidants 8(10):438. doi:10.3390/antiox8100438
2019
Aliaño-González, M. J., Ferreiro-González, M., Espada-Bellido, E., Palma, M., & Barbero, G. F. A screening method based on Visible-NIR spectroscopy for the identification and quantification of different adulterants in high-quality honey. (2019) Talanta 203: 235-241. doi:10.1016/j.talanta.2019.05.067
2019
Fernández-Barbero, G., Pinedo, C., Espada-Bellido, E., Ferreoro-Gonzales, M., Carrera, C., Palma, M., García-Barroso, C. Optimization of ultrasound-assisted extraction of bioactive compounds from jabuticaba (Myrciaria cauliflora) fruit through a box-behnken experimental design. (2019) Food Science and Technology DOI: 10.1590/fst.16918
2019
González-de-Peredo, A. V., Vázquez-Espinosa, M., Espada-Bellido, E., Ferreiro-González, M., Amores-Arrocha, A., Palma, M., F. Barbero, G., Jiménez-Cantizano, A. Discrimination of Myrtle Ecotypes from Different Geographic Areas According to Their Morphological Characteristics and Anthocyanins Composition. (2019). Plants, 8(9), 328. doi:10.3390/plants8090328
2019
Vázquez-Espinosa, M., V. González-de-Peredo, A., Espada-Bellido, E., Ferreiro-González, M., Toledo-Domínguez, J. J., Carrera, C., Palma, M. F. Barbero, G. Ultrasound-Assisted Extraction of Two Types of Antioxidant Compounds (TPC and TA) from Black Chokeberry (Aronia melanocarpa L.): Optimization of the Individual and Simultaneous Extraction Methods. (2019). Agronomy, 9(8), 456. doi:10.3390/agronomy9080456 
2019
Setyaningsih, W., Saputro, I.E., Carrera, C.A., Palma, M. Optimisation of an ultrasound-assisted extraction method for the simultaneous determination of phenolics in rice grains.(2019) Food Chemistry, 288, pp. 221-227
2019
Aliaño-González, M.J., Ferreiro-González, M., Barbero, G.F., Palma, M. Novel method based on ion mobility spectrometry sum spectrum for the characterization of ignitable liquids in fire debris (2019) Talanta, 199, pp. 189-194
2019
Vázquez-León, L. A., Olguín-Rojas, J. A., Páramo-Calderón, D. E., Palma, M., Barbero, G. F., Robles-Olvera, V. J., García-Alvarado, M.A., Rodríguez-Jimenes, G. C. Modeling of counter-current multistage extraction of Moringa oleifera leaves using a mechanistic model. (2019) Food and Bioproducts Processing, 115, 165–174. doi:10.1016/j.fbp.2019.04.003 
2019
Aliaño-González, M.J., Ferreiro-González, M., Espada-Bellido, E., Palma, M., Barbero, G.F.. A Screening Method Based on Headspace-Ion Mobility Spectrometry to Identify Adulterated Honey. (2019. Sensors (Basel) 19(7):1621. doi:10.3390/s19071621
2019
Ferreiro-González, M., Ruiz-Rodríguez, A., Barbero, G.F., Ayuso, J., Álvarez, J.A., Palma, M., Barroso, C.G. FT-IR, Vis spectroscopy, color and multivariate analysis for the control of ageing processes in distinctive Spanish wines.(2019) Food Chemistry, 277, pp. 6-11.
2019
Vázquez-Espinosa, M., V. González de Peredo, A., Ferreiro-González, M., Carrera, C., Palma, M., F. Barbero, G., & Espada-Bellido, E. Assessment of Ultrasound Assisted Extraction as an Alternative Method for the Extraction of Anthocyanins and Total Phenolic Compounds from Maqui Berries (Aristotelia chilensis (Mol.) Stuntz). (2019). Agronomy, 9(3), 148. doi:10.3390/agronomy9030148
2019
Vázquez-Espinosa, M., González de Peredo, A.V., Ferreiro-González, M., Carrera, C., Palma, M., Barbero, G.F., Espada-Bellido, E. Progression of the Total and Individual Capsaicinoids Content in the Fruits of Three Different Cultivars of Capsicum chinense Jacq. (2019).  Agronomy, 9(3), 141. doi:10.3390/agronomy9030141
2019
Setyaningsih, W., Saputro, I.E., Carrera, C.A., Palma, M., García-Barroso, C. Fast Determination of Phenolic Compounds in Rice Grains by Ultraperformance Liquid Chromatography Coupled to Photodiode Array Detection: Method Development and Validation (2019) Journal of Agricultural and Food Chemistry, 67 (10), pp. 3018-3027
2019
Espada-Bellido, E., Ferreiro-González, M., Carrera, C., Palma, M., Álvarez, J. A., F. Barbero, G., & Ayuso, J. (2019). Extraction of Antioxidants from Blackberry (Rubus ulmifolius L.): Comparison between Ultrasound- and Microwave-Assisted Extraction Techniques. Agronomy, 9(11), 745. doi:10.3390/agronomy9110745
2019
González de Peredo, A.V., Vázquez-Espinosa, M., Espada-Bellido, E., Ferreiro-González, M., Amores-Arrocha, A., Palma, M., Barbero, G.F., Jiménez-Cantizano, A. Alternative Ultrasound-Assisted Method for the Extraction of the Bioactive Compounds Present in Myrtle (Myrtus communis L.). (2019) Molecules, art. no. 882
2018
Estudio del efecto terapéutico del Limonastrium monopetalum para el tratamiento de la esclerosis múltiple. I Congreso de Jóvenes Investigadores del Mar. Poster. 03/10/2018 - 05/10/2018. Cádiz (Andalucía, España). Torres-Sánchez, Sonia; GARCÍA-PARTIDA, JOSÉ ANTONIO; Fernández-Ponce, María Teresa; Casas-Cardoso, Lourdes; Berrocoso-Domínguez, Esther M; Bravo-García, Lidia
2018
González de Peredo, A.V., Vázquez-Espinosa, M., Espada-Bellido, E., Jiménez-Cantizano, A., Ferreiro-González, M., Amores-Arrocha, A., Palma, M., Barroso, C.G., Barbero, G.F. Development of new analytical microwave-assisted extraction methods for bioactive compounds from myrtle (myrtus communis L.). (2018) Molecules, 23 (11), art. no. 2992
2018
Vázquez-Espinosa, M., Espada-Bellido, E., De Peredo, A.V.G., Ferreiro-González, M., Carrera, C., Palma, M., Barroso, C.G., Barbero, G.F. Optimization of microwave-assisted extraction for the recovery of bioactive compounds from the chilean superfruit (aristotelia chilensis (Mol.) Stuntz). (2018) Agronomy, 8 (11)
2018
Ferreiro-González, M., Espada-Bellido, E., Guillén-Cueto, L., Palma, M., Barroso, C.G., Barbero, G.F. Rapid quantification of honey adulteration by visible-near infrared spectroscopy combined with chemometrics. (2018) Talanta, 188, pp. 288-292
2018
Aliaño-González, M., Ferreiro-González, M., Barbero, G., Palma, M., & Barroso, C. (2018). Application of Headspace Gas Chromatography-Ion Mobility Spectrometry for the Determination of Ignitable Liquids from Fire Debris. Separations, 5(3), 41. doi:10.3390/separations5030041 
2018
Espada-Bellido, E., Ferreiro-González, M., Barbero, G.F., Carrera, C., Palma, M., Barroso, C.G. Alternative Extraction Method of Bioactive Compounds from Mulberry (Morus nigra L.) Pulp Using Pressurized-Liquid Extraction (2018) Food Analytical Methods, 11 (9), pp. 2384-2395. Cited 2 times
2018
Aliaño-González, M.J., Ferreiro-González, M., Barbero, G.F., Ayuso, J., Álvarez, J.A., Palma, M., Barroso, C.G. An electronic nose based method for the discrimination of weathered petroleum-derived products (2018) Sensors (Switzerland), 18 (7), art. no. 2180
2018
Ferreiro-González, M., Aliaño-González, M.J., Barbero, G.F., Palma, M., Barroso, C.G. Characterization of petroleum-based products in water samples by HS-MS (2018) Fuel, 222, pp. 506-512. Cited 2 times
2018
Falatová, B., Ferreiro-González, M., Martín-Alberca, C., Kačíková, D., Galla, Š., Palma, M., Barroso, C.G. Effects of fire suppression agents and weathering in the analysis of fire debris by HS-MS enose (2018) Sensors (Switzerland), 18 (6), art. no. 1933
2018
Stipcovich, T., Barbero, G.F., Ferreiro-González, M., Palma, M., Barroso, C.G. Fast analysis of capsaicinoids in Naga Jolokia extracts (Capsicum chinense) by high-performance liquid chromatography using fused core columns. (2018) Food Chemistry, 239, pp. 217-224. Cited 8 times
2018
Aliaño-González, M.J., Ferreiro-González, M., Barbero, G.F., Ayuso, J., Palma, M., Barroso, C.G. Study of the weathering process of gasoline by eNose(2018) Sensors (Switzerland), 18 (1), art. no. 139, . Cited 2 times
2018
Fayos, O., Barbero, G.F., Savirón, M., Orduna, J., Durán, A.G., Palma, M., Molinillo, J.M.G., Macías, F.A., Barroso, C.G., Mallor, C., Garcés-Claver, A. Synthesis of (±)-3,4-dimethoxybenzyl-4-methyloctanoate as a novel internal standard for capsinoid determination by HPLC-ESI-MS/MS(QTOF)(2018) Open Chemistry, 16 (1), pp. 87-94. Cited 2 times.
2017
Ferreiro-González, M., Barbero, G.F., Palma, M., Ayuso, J., Álvarez, J.A., Barroso, C.G. Characterization and differentiation of petroleum-derived products by E-nose fingerprints (2017) Sensors (Switzerland), 17 (11), art. no. 2544, . Cited 5 times
2017
Setyaningsih, W., Saputro, I.E., Carrera, C.A., Palma, M., Barroso, C.G. Multiresponse optimization of a UPLC method for the simultaneous determination of tryptophan and 15 tryptophan-derived compounds using a Box-Behnken design with a desirability function. (2017) Food Chemistry, 225, pp. 1-9. Cited 8 times
2017
Ruiz-Rodríguez, A., Carrera, C.A., Setyaningsih, W., Barbero, G.F., Ferreiro-González, M., Palma, M., Barroso, C.G. Tryptophan levels during grape ripening: Effects of cultural practices. (2017) Molecules, 22 (6), art. no. 941, . Cited 1 time
2017
Fayos, O., De Aguiar, A.C., Jiménez-Cantizano, A., Ferreiro-González, M., Garcés-Claver, A., Martínez, J., Mallor, C., Ruiz-Rodríguez, A., Palma, M., Barroso, C.G., Barbero, G.F. Ontogenetic variation of individual and total capsaicinoids in Malagueta peppers (Capsicum frutescens) during fruit maturation (2017) Molecules, 22 (5), art. no. 736, . Cited 6 times
2017
Setyaningsih, W., Saputro, I.E., Palma, M., Barroso, C.G. Optimization of the ultrasound-assisted extraction of tryptophan and its derivatives from rice (Oryza sativa) grains through a response surface methodology (2017) Journal of Cereal Science, 75, pp. 192-197. Cited 1 time
2017
Piñeiro, Z., Marrufo-Curtido, A., Vela, C., Palma, M. Microwave-assisted extraction of stilbenes from woody vine material (2017) Food and Bioproducts Processing, 103, pp. 18-26. Cited 3 times
2017
Ferreiro-González, M., Barbero, G.F., Ayuso, J., Álvarez, J.A., Palma, M., Barroso, C.G. Validation of an HS-MS method for direct determination and classification of ignitable liquids (2017) Microchemical Journal, 132, pp. 358-364. Cited 5 times.
2017
Ferreiro-González, M., Barbero, G.F., Álvarez, J.A., Ruiz, A., Palma, M., Ayuso, J. Authentication of virgin olive oil by a novel curve resolution approach combined with visible spectroscopy (2017) Food Chemistry, 220, pp. 331-336. Cited 14 times
2017
Espada-Bellido, E., Ferreiro-González, M., Carrera, C., Palma, M., Barroso, C.G., Barbero, G.F. Optimization of the ultrasound-assisted extraction of anthocyanins and total phenolic compounds in mulberry (Morus nigra) pulp (2017) Food Chemistry, 219, pp. 23-32. Cited 43 times
2017
De Souza Dias, F., Lovillo, M.P., Barroso, C.G., Carneiro, A.F., David, J.M. Direct determination of phenolic acids and hydroxymethylfurfural in wines elaborated in Vale do São Francisco region-Brazil by HPLC DAD (2017) Analytical Methods, 9 (4), pp. 643-648. Cited 2 times
2016
Setyaningsih, W., Hidayah, N., Saputro, I.E., Palma, M., García Barroso, C. Profile of phenolic compounds in Indonesian rice (Oryza sativa) varieties throughout post-harvest practices (2016) Journal of Food Composition and Analysis, 54, pp. 55-62. Cited 1 time
2016
Barbero, G.F., de Aguiar, A.C., Carrera, C., Olachea, Á., Ferreiro-González, M., Martínez, J., Palma, M., Barroso, C.G. Evolution of Capsaicinoids in Peter Pepper (Capsicum annuum var. annuum) During Fruit Ripening (2016) Chemistry and Biodiversity, pp. 1068-1075. Cited 3 times
2016
Setyaningsih, W., Saputro, I. E., Palma, M., & Barroso, C. G. (2016). Profile of individual phenolic compounds in rice (Oryza sativa) grains during cooking processes. doi:10.1063/1.4958556 
2016
Setyaningsih, W., Saputro, I. E., Palma, M., & Barroso, C. G. (2016). Stability of 40 phenolic compounds during ultrasound-assisted extractions (UAE). doi:10.1063/1.4958517
2016
Setyaningsih, W., Saputro, I.E., Palma, M., Barroso, C.G. Pressurized liquid extraction of phenolic compounds from rice (Oryza sativa) grains (2016) Food Chemistry, 192, art. no. 17784, pp. 452-459. Cited 16 times
2016
Piñeiro, Z., Marrufo-Curtido, A., Serrano, M.J., Palma, M. Ultrasound-assisted extraction of stilbenes from grape canes (2016) Molecules, 21 (6), art. no. 784, . Cited 7 times
2016
Ferreiro-González, M., Barbero, G.F., Palma, M., Ayuso, J., Álvarez, J.A., Barroso, C.G. Determination of ignitable liquids in fire debris: Direct analysis by electronic nose (2016) Sensors (Switzerland), 16 (5), art. no. 695, . Cited 12 times
2016
Barbero, G.F., Liazid, A., Azaroual, L., Palma, M., Barroso, C.G. Capsaicinoid Contents in Peppers and Pepper-Related Spicy Foods (2016) International Journal of Food Properties, 19 (3), pp. 485-493. Cited 16 times
2016
Coutinho, J.P., Barbero, G.F., Godoy, H.T., Palma, M., Barroso, C.G. Multivariate optimization by statistical methods of ultra high performance liquid chromatography conditions for the separation of 17 capsaicinoids (2016) Analytical Methods, 8 (7), pp. 1659-1666. Cited 2 times
2016
Setyaningsih, W., Duros, E., Palma, M., Barroso, C.G. Optimization of the ultrasound-assisted extraction of melatonin from red rice (Oryza sativa) grains through a response surface methodology (2016) Applied Acoustics, 103, pp. 129-135. Cited 8 times. 
2016
Guamán-Balcázar, M.C., Setyaningsih, W., Palma, M., Barroso, C.G. Ultrasound-assisted extraction of resveratrol from functional foods: Cookies and jams (2016) Applied Acoustics, 103, pp. 207-213. Cited 13 times
2016
Barbero, G.F., Liazid, A., Ferreiro-González, M., Palma, M., Barroso, C.G. Fast separation of capsaicinoids from peppers by reversed phase ultra-performance liquid chromatography: Comparation with traditional high-performance liquid chromatography methods (2016) International Journal of Food Properties, 19 (5), pp. 984-992. Cited 6 times
2015
Ferreiro-González, M., Ayuso, J., Álvarez, J.A., Palma, M., Barroso, C.G. Application of an HS-MS for the detection of ignitable liquids from fire debris (2015) Talanta, 142, pp. 150-156. Cited 13 times
2015
Ferreiro-González, M., Ayuso, J., Álvarez, J.A., Palma, M., Barroso, C.G. Gasoline analysis by headspace mass spectrometry and near infrared spectroscopy (2015) Fuel, 153, art. no. 9085, pp. 402-407. Cited 15 times
2015
Coutinho, J.P., Barbero, G.F., Avellán, O.F., Garcés-Claver, A., Godoy, H.T., Palma, M., Barroso, C.G. Use of multivariate statistical techniques to optimize the separation of 17 capsinoids by ultra performance liquid chromatography using different columns (2015) Talanta, 134, pp. 256-263. Cited 8 times
2015
Setyaningsih, W., Saputro, I.E., Palma, M., Barroso, C.G. Optimisation and validation of the microwave-assisted extraction of phenolic compounds from rice grains (2015) Food Chemistry, 169, pp. 141-149. Cited 29 times.
2015
Setyaningsih, W., Saputro, I.E., Barbero, G.F., Palma, M., García Barroso, C. Determination of melatonin in rice (Oryza sativa) grains by pressurized liquid extraction (2015) Journal of Agricultural and Food Chemistry, 63 (4), pp. 1107-1115. Cited 12 times
2015
Carrera, C., Ruiz-Rodríguez, A., Palma, M., Barroso, C.G. Ultrasound-assisted extraction of amino acids from grapes (2015) Ultrasonics Sonochemistry, 22, pp. 499-505. Cited 24 times