Yield Optimization and Supercritical CO2 Extraction of Essential Oil from Jasmine Flower

https://doi.org/10.22146/ijc.39710

Hesham Hussein Rassem(1*), Abdurahman Hamid Nour(2), Rosli Mohammad Yunus(3), Yasmeen Hafiz Zaki(4), Hybat Salih Mohamed Abdlrhman(5)

(1) Faculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, 26300 Gambang, Pahang, Malaysia
(2) Faculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, 26300 Gambang, Pahang, Malaysia
(3) Faculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, 26300 Gambang, Pahang, Malaysia
(4) Faculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, 26300 Gambang, Pahang, Malaysia
(5) Faculty of Chemical and Natural Resources Engineering, Universiti Malaysia Pahang, 26300 Gambang, Pahang, Malaysia
(*) Corresponding Author

Abstract


Supercritical fluid extraction (SFE) is an innovation that permits extraction of an extensive variety of different chemical composition from the plant grids. Extraction of essential oil from Jasmine flower was tentatively carried out using the supercritical CO2 technique. The effect of extraction parameters which include pressure (100–300 bar) and temperature (300–350 K) on the oil recovery was explored. The extraction process was optimized using the response surface methodology (RSM). At the SFE optimal conditions, the chemical compositions of the extracted oil were examined using gas chromatography-mass spectrometry (GC-MS) analysis. The obtained result reflected that the optimal yield of oil from Jasmine flower was 12.18% mg oil extracted/100 g dry flower, which was achieved through an SFE optimal conditions of pressure at 200 bar and extraction temperature at 325 K. A total number of six chemical compounds were tentatively identified in the Jasmine flower extracted oil at the optimal SFE conditions.

Keywords


jasmine flower; response surface methodology (RSM); essential oil; supercritical fluid; gas chromatography-mass spectrometry (GC-MS)

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References

[1] Burt, S., 2004, Essential oils: Their antibacterial properties and potential applications in foods—a review, Int. J. Food Microbiol., 94 (3), 223–253.

[2] Younis, A., Riaz, A., Khan, M.A., Khan, A.A., and Pervez, M.A., 2008, Extraction and identification of chemical constituents of the essential oil of Rosa species, Proc. XXVII-S5 Ornamental, Now!, 766, 485–492.

[3] Formaceck, V., and Kubeczka, K. H., 1982, Essential Oil by Capillary Gas Chromatography and Carbon 13 NMR Spectroscopy, John Wiley and Sons, 341–348.

[4] Oussalah, M., Caillet, S., Saucier, L., and Lacroix, M., 2006, Antimicrobial effects of selected plant essential oils on the growth of a Pseudomonas putida strain isolated from meat, Meat Sci., 73 (2), 236–244.

[5] Oussalah, M., Caillet, S., Saucier, L., and Lacroix, M., 2007, Inhibitory effects of selected plant essential oils on the growth of four pathogenic bacteria: E. coli O157:H7, Salmonella Typhimurium, Staphylococcus aureus and Listeria monocytogenes, Food Control, 18 (5), 414–420.

[6] Green, P., and Miller, D., 2009, The genus Jasminum in Cultivation, Royal Botanic Gardens, UK.

[7] Lawless, J., 2013, The Encyclopedia of Essential Oils: The Complete Guide to the Use of Aromatic Oils in Aromatherapy, Herbalism, Health, and Well Being, 1st ed., Conari Press, Newburyport, Massachusetts.

[8] Lawless, J., 1995, The Illustrated Encyclopedia of Essential Oils: The Complete Illustrated Guide to the Use of Oils in Aromatherapy and Herbalism, Element Books, Ltd., Shaftesbury, Dorset, UK.

[9] Mojay, G., 1999, Aromatherapy for Healing the Spirit: Restoring Emotional and Mental Balance with Essential Oils, Inner Traditions-Bear & Co., Rochester, Vermont, US.

[10] Reverchon, E., 1997, Supercritical fluid extraction and fractionation of essential oils and related products, J. Supercrit. Fluids, 10 (1), 1–37.

[11] Zizovic, I., Stamenić, M., Orlović, A., and Skala, D., 2007, Supercritical carbon dioxide extraction of essential oils from plants with secretory ducts: Mathematical modelling on the micro-scale, J. Supercrit. Fluids, 39 (3), 338–346.

[12] Carvalho, R.N., Moura, L.S., Rosa, P.T.V., and Meireles, M.A.A., 2005, Supercritical fluid extraction from rosemary (Rosmarinus officinalis): Kinetic data, extract's global yield, composition, and antioxidant activity, J. Supercrit. Fluids, 35 (3) 197–204.

[13] Meireles, M.A.A., 2003, Supercritical extraction from solid: process design data (2001–2003), Curr. Opin. Solid State Mater. Sci., 7 (4-5), 321–330.

[14] Özkal, S., Yener, M., and Bayındırlı, L., 2005, Response surfaces of apricot kernel oil yield in supercritical carbon dioxide, LWT Food Sci. Technol., 38 (6), 611–616.

[15] Zermane, A., Larkeche, O., Meniai, A.H., Crampon, C., and Badens, E., 2014, Optimization of essential oil supercritical extraction from Algerian Myrtus communis L. leaves using response surface methodology, J. Supercrit. Fluids, 85, 89–94.

[16] Md Zaidul, I.S., Nik Norulaini, N.A., and Mohd Omar, A.K., 2006, Separation/fractionation of triglycerides in terms of fatty acid constituents in palm kernel oil using supercritical CO2, J. Sci. Food Agric., 86 (7), 1138–1145.

[17] Larkeche, O., Zermane, A., Meniai, A.H., Crampon, C., and Badens, E., 2015, Supercritical extraction of essential oil from Juniperus communis L. needles: Application of response surface methodology, J. Supercrit. Fluids, 99, 8–14.

[18] Reverchon, E., and Osséo, L.S., 1994, Comparison of processes for the supercritical carbon dioxide extraction of oil from soybean seeds, J. Am. Oil Chem. Soc., 71 (9), 1007–1012.

[19] Zermane, A., Meniai, A.H., and Barth, D., 2010, Supercritical CO2 extraction of essential oil from Algerian rosemary (Rosmarinus officinalis L.), Chem. Eng. Technol., 33 (3), 489–498.

[20] Calvo, L., Cocero, M., and Díez, J., 1994, Oxidative stability of sunflower oil extracted with supercritical carbon dioxide, J. Am. Oil Chem. Soc., 71 (11), 1251–1254.

[21] Salgın, U., 2007, Extraction of jojoba seed oil using supercritical CO2+ethanol mixture in green and high-tech separation process, J. Supercrit. Fluids, 39 (3), 330–337.

[22] Xu, J., Chen, S., and Hu, Q., 2005, Antioxidant activity of brown pigment and extracts from black sesame seed (Sesamum indicum L.), Food Chem., 91 (1), 79–83.

[23] Papamichail, I., Louli, V., and Magoulas, K., 2000, Supercritical fluid extraction of celery seed oil, J. Supercrit. Fluids, 18 (3), 213–226.

[24] Louli, V., Folas, G., Voutsas, E., and Magoulas, K., 2004, Extraction of parsley seed oil by supercritical CO2, J. Supercrit. Fluids, 30 (2), 163–174.

[25] Marrone, C., Poletto, M., Reverchon, E., Stassi, A., 1998, Almond oil extraction by supercritical CO2: Experiments and modelling, Chem. Eng. Sci., 53 (21), 3711–3718.

[26] Palazoglu, T.K., and Balaban, M.O., 1998, Supercritical CO2 extraction of lipids from roasted pistachio nuts, Trans. ASAE, 41 (3), 679–684.

[27] Haloui, I., and Meniai, A.H., 2017, Supercritical CO2 extraction of essential oil from Algerian Argan (Argania spinosa L.) seeds and yield optimization, Int. J. Hydrogen Energy, 42 (17), 12912–12919.

[28] Pereda, S., Bottini, S.B., and Brignole, E.A., 2008, “Fundamentals of Supercritical Fluid Technology” in. Supercritical Fluid Extraction of Nutraceuticals and Bioactive Compounds, Eds., Martinez, J.L., CRC Press, 1–24.

[29] Roy, B.C., Goto, M., and Hirose, T., 1996, Extraction of ginger oil with supercritical carbon dioxide: Experiments and modeling. Ind. Eng. Chem. Res., 35 (2), 607–612.

[30] Zhu, T., Heo, H.J., and Row, K.H., 2012, Central composite design for optimized extraction of polysaccharides from Undaria pinnatifida, Chem. Res. Chin. Univ., 28 (4), 620–623.



DOI: https://doi.org/10.22146/ijc.39710

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