Research article
Vol 0 No 0.1 (3000): ONLINE FIRST
Different concentrations and solubility of active lime (CaCO3) on the quality of indigo paste from Indigofera longiracemosa Boiv.ex. Baill
Department of Biology Education, Faculty of Teacher Training and Education, Universitas Sebelas Maret
Universitas Sebelas Maret
Abstract
This research aims to determine the effect of differences in concentration and solubility of active lime (25% and 35% CaCO3 solution, 25% and 35% CaCO3 supernatant) on the quality of indigo (Indigofera longiracemosa) dye paste. The method for making indigo dye paste includes the process of soaking fresh leaves and twigs of I. longiracemosa in water, fermentation with an active lime solution of CaCO3 with varying concentrations and solubility, settling, and filtration to obtain indigo paste. Several tests were carried out to evaluate the quality of the color in the fabric and the indican content in the indigo produced. The indican content that was successfully tested showed the highest results in the paste treated with 25% CaCO3. Color quality tests on fabrics show that fabrics dyed with indigo paste with 35% CaCO3 solution treatment have the best color fastness to sweat with an average value of 4. The color fastness test to heat on fabric dyed with indigo paste with all types of treatment received a score of 4-5, which indicates excellent color fastness, does not fade, and does not stain other fabrics. The differences in concentration and solubility of CaCO3 solution result in variations in the physical characteristics of indigo paste, the colors produced on fabric, the indican content, as well as the colorfastness to sweat and heat.
References
- Aggarwal S. 2021. Indian dye yielding plants: Efforts and opportunities. Natural Resources Forum. 45(1):63–86. doi: 10.1111/1477-8947.12214.
- Alamsyah A. 2018. Kerajinan batik dan pewarnaan alami. Endogami: Jurnal Ilmiah Kajian Antropologi. 1(2):136. doi: 10.14710/endogami.1.2.136-148.
- Ariyanti M, Asbur Y. 2018. Tanaman tarum ( Indigofera tinctoria linn. ) sebagai penghasil zat pewarna. Jurnal Hutan Pulau-Pulau Kecil. 2(1):109–122. doi:10.30598/jhppk.2018.2.1.109.
- Arta TK, Atika V, Haerudin A, Isnaini I, Masiswo M. 2019. Kualitas pewarnaan batik menggunakan bubuk Indigofera tinctoria dan Strobilanthes cusia. Dinamika Kerajinan dan Batik: Majalah Ilmiah. 36(2):163. doi:10.22322/dkb .v36i2.5421.
- Chavan RB. 2015. Indigo dye and reduction techniques. In: Denim: Manufacture, Finishing and Applications. Elsevier. p. 37–67. doi:10.1016/B978-0-85709-843-6.000 03-2.
- Eskak E, Salma IR. 2020. Kajian pemanfaatan limbah perkebunan untuk substitusi bahan pewarna alami batik. Jurnal Industri Hasil Perkebunan. 15(2):27. doi:10.33104/jihp. v15i2.6331.
- Fried R, Oprea I, Fleck K, Rudroff F. 2022. Biogenic colourants in the textile industry – a promising and sustainable alternative to synthetic dyes. Green Chemistry. 24(1):13–35. doi:10.1039/d1gc02968a.
- Fugarasti H, Muzzazinah, Ramli M. 2020. Morphoanatomy of three indigofera species (Leguminosae-papilionoideae) in Java, Indonesia. Biodiversitas. 21(11):5531–5539. doi: 10.13057/biodiv/d211162.
- Haryanto D, Sasmita ER. 2019. Budidaya tanaman indigofera. LPPM UPN Veteran Yogyakarta. http://eprints.upnyk.ac.id/36175/#.
- Hossain MD, Khan MMR, Uddin MZ. 2017. Fastness properties and color analysis of natural indigo dye and compatibility study of different natural reducing agents. Journal of Polymers and the Environment. 25(4):1219–1230. doi: 10.1007/s10924-016-0900-6.
- Martuti NKT, Hidayah I, Margunani. 2019. Pemanfaatan indigo sebagai pewarna alami ramah lingkungan bagi pengrajin batik zie. Jurnal Pengabdian Kepada Masyarakat. 3(2):133–143. https://journal.unhas.ac.id/index.php/panritaabdi/article/view/6454/4225.
- Muzayyinah M. 2014. Indigofera: “Kini dan nanti”. Bioedukasi: Jurnal Pendidikan Biologi. 7(2):23. doi: 10.20961/bioeduk asi-uns.v7i2.2932.
- Muzayyinah M. 2016. Ethnobotany of indigofera in Indonesia. Bioedukasi: Jurnal Pendidikan Biologi. 9(2):7. doi: 10.209 61/bioedukasi-uns.v9i2.4000.
- Muzzazinah, Chikmawati T, Ariyanti NS. 2016. Correlation of morphological characteristics with the presence of indicant in indigofera sp. Dyestuff. Sains Malaysiana. 45(6):883–890. https://ukm.my/jsm/pdf_files/SM-PDF-45-6-2016/05Muzzazinah.pdf.
- Muzzazinah, Chikmawati T, Sri Ariyanti N. 2015. Indigofera longeracemosa boiv. ex baill. di Jawa. Floribunda. 5(3):106–110. http://www.ptti.or.id/journal/index.php/Floribunda/article/view/7.
- Muzzazinah, Suratman, Nurmiyati, Ariani SRD. 2021. Morphological and anatomical characters variation of Indigofera accessions from Java, Indonesia. Biodiversitas. 22(4):2104–2116. doi: 10.13057/biodiv/d220459.
- Pujilestari T. 2017. Optimasi pencelupan kain batik katun dengan pewarna alam tingi (Ceriops tagal) dan Indigofera sp. Dinamika Kerajinan dan Batik: Majalah Ilmiah. 34(1):53. doi: 10.22322/dkb.v34i1.2606.
- Purnama H, Hidayati N, Safitri DS, Rahmawati S. 2017. Effect of initial treatment in the preparation of natural indigo dye from Indigofera tinctoria. AIP Conference Proceedings. Volume 1855. p. 1–6. doi: 10.1063/1.4985467.
- Purwanto. 2018. Hasil uji beda warna bahan alami sebagai salah satu alternatif pewarnaan pada bahan kain batik. Jurnal Rekarupa. 5(Vol 5, No 1 (2018)):54–61. https://ejurnal.itenas.ac.id/index.php/rekarupa/article/view/2370/1862.
- Putri AWA, Angelica J, Kartawidjaja K. 2021. Pewarnaan dan pemberian motif alami kain celup ikat itajime shibori dengan ekstrak indigofera dan tunjung. Gorga : Jurnal Seni Rupa. 10(2):541. doi: 10.24114/gr.v10i2.28490.
- Saikhao L, Kaew-unruan N, Thanomsith K, Dulyasucharit R, Munmuangsan W. 2025. A study of the influence of the addition of lime to natural indigo production. Applied Surface Science. 689(162474):162474. doi:10.1016/j.apsu sc.2025.162474.
- Singh K, Kumar P, Singh NV. 2020. Natural dyes: An emerging ecofriendly solution for textile industries. Poll Res. 39(February):87–94. https://www.envirobiotechjournals.com/PR/FebSupplIssue2020/PollRes-13.pdf.
- Siregar AH. 2017. Pembuatan zat warna alam dari tumbuhan berasal dari daun. Bina Teknika. 12(1):103. doi: 10.54378/bt.v12i1.96.