PREPARASI DAN PENENTUAN JENIS OKSIDA BESI PADA MATERIAL MAGNETIK PASIR BESI LANSILOWO

https://doi.org/10.22146/teknosains.11385

Ricka Prasdiantika(1*), Susanto Susanto(2)

(1) Fakultas Teknik Universitas Pandanaran Semarang
(2) Fakultas Teknik Universitas Pandanaran Semarang
(*) Corresponding Author

Abstract


This study aims to preparation, identify the content, and determine the type of iron oxide on the magnetic material from Iron Sand Lansilowo. Magnetic material is separated from iron sand using an external magnet. Magnetic material washes by using aquadest and dried at 80 °C. Materials were characterized by X-Ray fluorescence (XRF), Fourier Transform Infrared (FT-IR) spectrophotometer, X-ray diffractometer (XRD) and Transmission electron microscope (TEM). The results show that the magnetic material of iron sand Lansilowo contains elements of Fe (46.13%), the element Cr (28.08%), Mg (10,11%), Si (8.20%) and other minor elements. Iron oxide contained in iron sand Lansilowo is dominated by magnetite iron oxide (Fe3O4). The results of characterization show that the magnetic material of iron sand still contain oxide impurities such as silica oxide and chromium oxide


Keywords


Magnetite;Magnetic material; Iron oxide; Iron sand; Preparation

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References

Yang, L., G. Xi, T. Lou, X. Wang, J. Wang, and Y. He. 2016. Preparation and Magnetic Performance of Co0.8 Fe2.2O4 by A Sol-gel Method Using Cathode Materials of Spent Li-ion Batteries. Ceramics International Part B 42(1): 1897-1902.

Jiang, F., X. Wang, and D. Wu. 2016. Magnetic Microencapsulated Phase Change Materials With An Organo-Silica Shell: Design, Synthesis and Application For Electromagnetic Shielding and Thermal Regulating Polymide Films. Energy 98: 225-239

Pang, Y.L., S. Lim, H.C. Ong, and W.T. Chong. 2016. Research Progress on Iron Oxide-based Magnetic Materails: Synthesis Techniques and Photocatalytic Applications (Review Article). Ceramics International Part A 42(1): 9-34.

Cohen, S., A. Deodhar, A. Kavanaugh, E. Ruderman, R.H. Shmerling, B.N. Weissman, M. Weisman, and C. Winalski. 2006. Extremity Magnetic Resonance Imaging in Rheumatoid Arthritis. Arthritis & Rheumatism 54(4): 1034-1047.

Anwar, N. 2011. Pembuatan Magnet Permanen Nd2Fe14B Melalui Metode Mechanical Alloying. Skripsi. Program Studi Fisika Universitas Islam Negeri Syarif Hidayatullah. Jakarta.

Hunt, C.P., B.M. Moskowitz, and S.K. Banerjee. 1995. Magnetic Properties of Rocks and American Minerals. Rock Physics & Phase Relations: A Handbook of Physical Constants. Geophysical Union: 189-204.

Mahdavi, M., M.B. Ahmad, M.J. Haron, F. Namvar, B. Nadi, M.ZA. Rahman, and J. Amin. 2013. Synthesis, Surface Modification and Characterization of Biocompatible Magnetic Iron Oxide Nanoparticles for Biomedical Application. Molecules 18: 7533-7548.

Chougale, U.M. and V.J. Fulari. 2014. Facile Synthesis of Maghemite Nanoflakes Arrays for Supercapasitor Application. Materials Science in Semiconductor Processing 27: 682-688.

Ge, F., L. Meng-Meng, Y. Hui, and Z. Bao-Xiang. 2012. Effective Removal of Heavy Metal Ions Cd2+, Zn2+, Pb2+, Cu2+ from Aqueous Solution by Polymer-Modified Magnetic Nanoparticles. Journal of Hazardous Materials 211-212: 366-372.

Legodi, M.A. and D.de Waal. 2007. The Preparation of Magnetite, Geothite, Hematite and Maghemite of Pigment Quality from Mill Scale Iron Waste. Dyes and Pigments 74: 161-168.

Zhang, Y., Q. Xu, S. Zhang, J. Liu, J. Zhou, H. Xu, H. Xiao, and J. Li. 2013. Preparation of Thiol-modified Fe3O4@SiO2 Nanoparticles and Their Application for Gold Recovery from Dilute Solution. Separation Purification Technology 116: 391–397.

Iida H., K. Takayanagi, T. Nakanishi, and T. Osaka. 2007. Synthesis of Fe3O4 Nanoparticles with Various Size and Magnetic Properties by Controlled Hydrolysis. Journal of Colloid and Interface Science 314: 274-280.

Chung, J., J. Chun, J. Lee, S.H Lee, Y.J Lee, and S.W. Hong. 2012. Sorption of Pb(II) and Cu(II) Onto Multi-amine Grafted Mesoporous Silica Embedded with Nano-Magnetite: Effects of Steric Factors. Journal of Hazardous Materials 239-240: 183-191.

Cornell, R.M. and U. Shwertmann. 2003. The Iron Oxide: Scructure, Properties, Reaction, Occurences and Use. 2nd ed. WILEY-VOH GmbH & Co. KGaA.

Komatina, M., W. Heinrich, and Gudenau. 2004. The Sticking Problem During Direct Reduction of Fine Iron Ore in The Fluidized Bed. Journal Metallurgy 3:309.

Mufit, F., H. Amir, Fadhilah, dan S. Bijaksana. 2013. Kaitan Sifat Magnetik dengan Tingkat Kehiataman (Darkness) Pasir Besi di Pantai Masang Sumatera Barat. Eksakta 2: 70-75.

Ansori, C. 2013. Mengoptimalkan Perolehan Mineral Magnetik pada Proses Separasi Magnetik Pasir Besi Pantai Selatan Kabupaten Kebumen Jawa Tengah. Jurnal Teknologi Mineral dan Batubara 9(3): 145-156.

Rahmawati, R. dan N. Handayani. 2013. Fabrikasi Ferrogel Berbahan Dasar Nanopartikel Magnetit (Fe3O4) dari Hasil Sintesis Pasir Besi Pantai Utara Jawa dan Sifat Magneto-Elastisitasnya. Kaunia IX(1): 70-82.

Suhandi, H. Susanto, dan R. Hutamadi. 2011. Penelitian Bahan Galian Lain dan Mineral Ikutan pada Wilayah Pertambangan Kabupaten Konawe, Provinsi Sulawesi Tenggara. Prosiding Hasil Kegiatan Pusat Sumber Daya Geologi: II.9.

Sufriadin, S. Widodo, dan R. Biatong. 2013. Karakterisasi Mineralogi Bijih Besi Laterit dan Potensinya Sebagai Bahan Baku Industri Besi Baja di Indonesia. Prosiding Hasil Penelitian Fakultas Teknik. Universitas Hasanuddin: 1-4.

Setiawati, L.D., T.P. Rahman, D.W. Nugroho, Nofrizal, R. Ikono, Suryandaru, Yuswono, Siswanto, dan N.T Rochman. 2013. Ekstraksi Titanium Dioksida (TiO2) dari Pasir Besi dengan Metode Hidrometalurgi. Prosiding Semirata FMIPA Universitas Lampung: 465-468.

Yulianto, A. 2007. Fasa Oksida Besi untuk Sintesis Serbuk Magnet Ferit. Indonesian Journal Material Science 8: 39-41.

Zulfalina, dan A. Manaf. 2004. Identifikasi Senyawa Mineral dan Ekstraksi Titanium Dioksida dari Pasir Mineral. Indonesian Journal Material Science 5: 46-50.

Bruce, I.J., J. Taylor, M. Todd, M.J. Davies, E. Borioni, C. Sangregorio, and T. Sen. 2004. Synthesis, Characteri-zation and Application of Silica-Magnetite Nanocomposites. Journal of Magnetism and Magnetic Materials 284: 145-160.

Yamaura, M., R. L. Camilo, L.C. Sampaio, M.A. Macedo, N. Nakamura, and Toma, H.E. 2004. Preparation and Characterization of (3-aminopropyl) triethoxysilane-coated Magnetite Nanoparticles. Journal of Magnetism and Magnetic Materials 279: 210-217.

Farimani, N.S., N.G. Roknabadi, and A. Kazemi. 2013. Study of Structural and Magnetic Properties of Superparamagnetic Fe3O4/SiO2 Core-Shell Nanocomposites Synthe-sized with Hydrophilic Citrate-Modified Fe3O4 Seeds Via A Sol-Gel Approach. Physica E 53: 207-216.

Petcharoen, K. and A. Sirivat. 2012. Synthesis and Characterization of Magnetite Nanoparticles Via The Chemical Co-Precipitation Method. Materials Science Engineering B 177: 421– 427.

Jal, P.K., M. Sudarshan, A. Saha, S. Patel, B.K. Mishra. 2004. Synthesis and Characterization of Nanosilica Prepared by Precipitation Method. Colloids and Surfaces A: Physicochemical Engineering Aspects 240: 173-178.

Saman, N., K.. Johari, and H. Mat. 2013. Adsorption Characteristics of Sulfur-Functionalized Silica Microspheres with Respect to the Removal of Hg(II) from Aqueous Solutions. Industrial and Engineering Chemistry Research 53: 1225-1233.

Zulkifli, N.S.C., I.A. Rahman, D. Mohamad, and A. Husein. 2013. A Green Sol-Gel Route For The Synthesis of Structurally Controled Silica Particles From Rice Husk for Dental Composie Filler. Ceramics International 39: 4559-4567.

Lakay, E. M.. 2009. Superparamagnetic Iron-Oxide Based Nanoparticles for The Separation and Recovery of Precious Metals from Solution. Thesis. University of Stellenbosch.

Montagne, F., O. Mondain-Monval, C. Pichot, H. Mozzanega, and Elaissari. 2002. Preparation and Characterization of Narrow Sized (O/W) Magnetic Emulsion. Journal of Magnetism and Magnetic Materials 250: 302-312.

Sulistyorini, L. 2014. Pelapisan Magnetit dengan Silika Termodifikasi Amino, Skripsi. Jurusan Kimia Universitas Gadjah Mada. Yogyakarta.

Wu, S., A. Sun, F. Zhai, J. Wang, W. Xu, Q. Zhang, and A.A. Volinsky. 2011. Fe3O4 Magnetic Nanoparticles Synthesis from Tailings by Ultrasonic Chemical Co-Precipitation. Materials Letters 65: 1882-1884.



DOI: https://doi.org/10.22146/teknosains.11385

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